LC/MS Report File D:\\DATA\\A02\\MONITOR\\CPK2016-713-108141-04479-LCMSA016.D Injection Date : 20 Jul 16 3:34 pm +0800 Tgt Mass(EZX) : 230.00 Sample Name : CPK2016-713-10814 Location : P1-C-06 Acq. Operator : A02-Monitor Inj : 1 Spec. Reported : MS Integration Inj Volume : 3 ul Acq. Method : D:\\METHODS\\1-POS-MON.M Analysis Method : D:\\METHODS\\1-POS-MON.M Catalog No : HY-13221 Batch#10814 Easy-Access Method: '1-POS-MON' 230.00 Method Info : Mobile Phase: A: water(0.01%TFA) B : ACN Gradient: 5%B increase to 95%B within1.5min, 95%B for 1.5min,back to 5%B within 0.01min. Flow Rate: 2.0 mL/min Column: Sunfire C18 4.6*50mm 3.5um Oven Temperature: 50 C Mass Range:103-1500*ADC1 A, ELSD mV23.2223.21800.5*DAD1 A, Sig=214,4 Ref=off 500000.5*DAD1 B, Sig=254,4 Ref=off 0.8330.83311.522.5min*mAU0.9371.39911.522.5min*mAU50000.51 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 700.8341.522.52.807min*200000100000000.51 Ion 231, MSD1 231,Target Mass 230 +H Positive, EIC=230.7:231.7 100000000.5 Integration Results for ADC1 A, ELSD10.2560.8341.522.5min1.522.5min RetTim Width Area Height Area%|-------|--------|--------------|--------------|--------| Integration Results for DAD1 A, Sig=214,4 Ref=off RetTim Width Area Height Area%|-------|--------|--------------|--------------|--------| 0.83 0.03 1535.23 980. 98.86 0.94 0.01 9.09 9.10 0.59 1.40 0.02 8.67 8.25 0.56 Integration Results for DAD1 B, Sig=254,4 Ref=off RetTim Width Area Height Area%|-------|--------|--------------|--------------|--------| 0.83 0.02 173.51 114.86 100.00LCMSA016 07/20/2016 3:37:38 PM A02-MonitorPage 1 of 2
LC/MS Report
Ret. Time: 0.83 <<<< POSITIVE SPECTRA >>>> ES-API Positive 231.1500004000030000 232.220000100000200400600800100012001400m/zRet. Time: 2.81 ES-API Positive180001600014000120001000080006000400020000 338.3 360.3 159.0 193.9 218.9 339.3 361.3 430.6200400600800100012001400m/zLCMSA016 07/20/2016 3:37:38 PM A02-MonitorPage 2 of 2
